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TRI-N-OCTYLALUMINIUM
  • Chemical Name:TRI-N-OCTYLALUMINIUM
  • CAS No.:1070-00-4

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1.What is the TRI-N-OCTYLALUMINIUM ?

Polyolefin catalyst.

aluminium hydride

aluminium hydride

oct-1-ene
111-66-0,25068-25-1

oct-1-ene

trioctylaluminum
1070-00-4

trioctylaluminum

Conditions
Conditions Yield
In octane; under N2 or Ar; suspn. of (AlH3)(n) in octane heated to 120°C; olefin (1 equiv.) added dropwise; after 30 min temp. raised to 125°C (reflux); cooled to 100-110°C; olefin (2.1 equiv.) added over 3-4 h; kept (90-100°C, 1 h); cooled; filtered through glass filter; solvent amd excess olefin distd. off in vac. below 80°C (7 Torr); elem. anal.;
91%
With triisobutylaluminum; In octane; under N2 or Ar; vertical ball mill loaded with (AlH3)(n), i-Bu3Al, olefin (molar ratio 1:0.14:4.8) and octane; heated gradually to 100°C with stirring; cooled; stored at 90-100°C for 2 h; balls and blend sepd.; residue washed with octane; filtrate evapd. at 80-90°C (7 Torr); elem. anal.;
88.6%
With Na(i-Bu)3AlH; In octane; under N2 or Ar; mixt. of (AlH3)(n), Na(i-Bu)3AlH (molar ratio 1:0.24) and octane heated to 80°C for 1 h; olefin added; temp. spontaneously raised to 100°C for 20 min; cooled; olefin additionally added dropwise at 90°C for 0.5-1 h; filtered; solvent and excess olefin distd. off in vac. below 80°C(7 Torr); mixt. of (C8H17)3Al and NaAl(C8H17)4 obtained; elem. anal.;
aluminum hydride
7784-21-6

aluminum hydride

oct-1-ene
111-66-0,25068-25-1

oct-1-ene

trioctylaluminum
1070-00-4

trioctylaluminum

Conditions
Conditions Yield
With lithium aluminium tetrahydride; aluminium trichloride; In octane; byproducts: LiCl; under N2 or Ar; mixt. of γ-AlH3, excess LiAlH4, octane and olefin heated to 100-110°C for 1 h; additional olefin added at 90-100°C for 2 h; filtered; solvent and excess olefin removed in vac. at 60-70°C (1Torr); AlCl3 added; heated at 80°C; filtered; elem. anal.;
89%

2.What is the CAS number for TRI-N-OCTYLALUMINIUM ?

The CAS number of TRI-N-OCTYLALUMINIUM is 1070-00-4.

More information of TRI-N-OCTYLALUMINIUM 1070-00-4 are:

CAS?Number

1070-00-4

Density

0.701 g/mL at 25 °C

Melting Point

<-40 °C

Boiling Point

126.4oC at 760mmHg

Flash Point

-6 °F

Vapor Pressure

1hPa at 25℃

HS CODE

29310099

PSA

0.00000

LogP

9.94350

3.What are another words for TRI-N-OCTYLALUMINIUM ?

Synonyms?for?TRI-N-OCTYLALUMINIUM 1070-00-4:Trioctylaluminum;Aluminum, trioctyl-;Trioctylalane;

4.What is the molecular formula of TRI-N-OCTYLALUMINIUM?

The chemical formula of ?TRI-N-OCTYLALUMINIUM is?C24H51Al which containing 24 Carbon atoms,51 Hydrogen atoms and 1 Aluminum atoms,and the molecular weight of??TRI-N-OCTYLALUMINIUM?is 366.65.

5.What is TRI-N-OCTYLALUMINIUM (1070-00-4) used for?

InChI:InChI=1/3C8H17.Al/c3*1-3-5-7-8-6-4-2;/h3*1,3-8H2,2H3;/rC24H51Al/c1-4-7-10-13-16-19-22-25(23-20-17-14-11-8-5-2)24-21-18-15-12-9-6-3/h4-24H2,1-3H3

Relevant articles related to TRI-N-OCTYLALUMINIUM:

Article

Source

One-step synthesis of trialkylaluminum derivatives and dialkylaluminum hydrides by the reaction of alkaline metal aluminum hydrides with α-olefins and alkylaluminum chlorides

Gavrilenko

, p. 168 - 169 (2003)

Insertion, elimination and isomerisation of olefins at alkylaluminium hydride: An experimental and theoretical study

Weliange, Nandita M.,McGuinness, David S.,Gardiner, Michael G.,Patel, Jim

, p. 15286 - 15296 (2015)

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