Home >Pharmaceutical > O-Mesitylenesulfonylhydroxylamine
- Chemical Name: O-Mesitylenesulfonylhydroxylamine
- CAS No.: 36016-40-7
Top quality factory supply 36016-40-7 O-Mesitylenesulfonylhydroxylamine at low price
- Molecular Formula: C9H13NO3S
- Molecular Weight: 215.273
- Vapor Pressure: 1.75E-06mmHg at 25°C
- Melting Point: 93-94 °C
- Refractive Index: 1.556
- Boiling Point: 350.587 °C at 760 mmHg
- PKA: -4.59±0.70(Predicted)
- Flash Point: 165.83 °C
- PSA： 77.77000
- Density: 1.24 g/cm3
- LogP: 2.97190
O-Mesitylenesulfonylhydroxylamine(Cas 36016-40-7) Usage
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Synthesis Reference(s) |
The Journal of Organic Chemistry, 38, p. 1239, 1973 DOI: 10.1021/jo00946a045Synthesis, p. 788, 1975 DOI: 10.1055/s-1975-23927 |
InChI:InChI=1/C9H13NO3S/c1-6-4-7(2)9(8(3)5-6)14(12,13)10-11/h4-5,10-11H,1-3H3
36016-40-7 Relevant articles
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, p. 67 - 76 (1989)
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36016-40-7 Process route
-
-
1239506-69-4
ethyl (1E)-N-(2,4,6-trimethylphenyl)sulfonyloxyethanimidate
-
-
36016-40-7
mesitylenesulfonylhydroxylamine
| Conditions | Yield |
|---|---|
|
With
perchloric acid;
In
1,4-dioxane;
at 0 ℃;
for 1.5h;
Inert atmosphere;
|
73%
|
|
With
perchloric acid;
In
1,4-dioxane;
at 0 ℃;
for 1.5h;
|
73%
|
|
With
perchloric acid;
In
1,4-dioxane;
at 0 ℃;
for 1.5h;
|
73%
|
|
With
perchloric acid;
In
1,4-dioxane;
ice-cooling;
|
|
|
With
perchloric acid;
In
1,4-dioxane;
at 0 ℃;
for 0.0833333h;
|
3.11 g
|
|
With
perchloric acid;
In
1,4-dioxane;
at 10 ℃;
Cooling with ice;
|
|
|
With
perchloric acid;
In
1,4-dioxane; water;
at 0 - 20 ℃;
for 1h;
|
|
|
With
perchloric acid;
In
1,4-dioxane;
at 0 - 20 ℃;
for 1.5h;
|
|
|
With
trifluoroacetic acid;
In
water;
at -5 ℃;
for 1.5h;
|
|
|
With
perchloric acid;
In
1,4-dioxane;
at 0 ℃;
for 0.75h;
|
|
|
With
perchloric acid;
In
1,4-dioxane;
at 0 ℃;
for 0.25h;
|
|
|
With
perchloric acid;
In
acetonitrile;
at 30 ℃;
for 0.25h;
Flow reactor;
|
|
|
With
water; trifluoroacetic acid;
at -5 ℃;
for 1.5h;
|
|
|
With
perchloric acid;
In
1,4-dioxane;
at 0 - 20 ℃;
for 1.5h;
|
|
|
With
perchloric acid;
In
1,4-dioxane;
at 0 ℃;
|
|
|
With
perchloric acid;
at 0 ℃;
for 1.08333h;
|
110 g
|
|
With
perchloric acid;
In
1,4-dioxane;
at 0 ℃;
for 0.166667h;
|
-
-
(Z)-ethyl N-(mesitylsulfonyl)oxyacetimidate
-
-
36016-40-7
mesitylenesulfonylhydroxylamine
| Conditions | Yield |
|---|---|
|
With
perchloric acid;
In
tetrahydrofuran; water;
at 0 - 5 ℃;
for 1.33333h;
Inert atmosphere;
|
81.3%
|
|
With
perchloric acid;
In
1,4-dioxane;
for 0.383333h;
Cooling;
Inert atmosphere;
|
|
|
With
perchloric acid; water;
In
tetrahydrofuran;
at 0 - 5 ℃;
for 1.5h;
Inert atmosphere;
|
36016-40-7 Upstream products
-
58658-55-2
O-(2,4,6-trimethylphenylsulfonyl)-N,N-bis(trimethylsilyl)hydroxylamine
-
38202-27-6
ethyl O-(2-mesitylenesulfonyl)acetohydroxamate
-
773-64-8
2-mesitylenesulphonyl chloride
-
36016-39-4
N-(tert-butoxycarbonyl)-O-(mesitylsulfonyl)hydroxylamine
36016-40-7 Downstream products
-
51578-86-0
2,3-diamino-thiazolium; 2,4,6-trimethyl-benzenesulfonate
-
53995-67-8
2,3-diamino-4-methyl-thiazolium; 2,4,6-trimethyl-benzenesulfonate
-
53995-64-5
3-amino-2-formylamino-thiazolium; 2,4,6-trimethyl-benzenesulfonate
-
52197-79-2
3-amino-2-methyl-benzothiazolium; 2,4,6-trimethyl-benzenesulfonate